Exported Data Example
This exported data has been truncated for this manual.
Copy
Sample Information
Method: $ CuO H2Ar TPR
Sample: CuO H2Ar TPR
Operator: PK
Submitter: Performance Test
Mass type: Calculated
Empty tube: 26.5221 g
Sample + tube: 26.5843 g
Sample mass: 0.0622 g
Density: 1.000 g/cm³
Type of data: Automatically collected
Instrument type: 2930
Original instrument type: 2930
Comments: Performance Test Run1
CuO Lot SZBG3070H
Sample+Tube mass after analysis: 26.5749g
Analysis Conditions
Analysis conditions: Analysis Conditions
View conditions for: AutoChem III 2930
Baseline Options
Stable Baseline
Slope threshold: 0.010 %/min
Duration: 5.00 min
Change from Baseline
Acceleration threshold: 0.200 %/min²
Duration: 0.10 min
Return to Baseline
Acceleration threshold: 0.050 %/min²
Duration: 1.00 min
Tasks
Description Details
1.01 Experiment --- CuO TPR 50 sccm H2Ar ---
Temperature Programmed
1.02 Instrument Settings --- Instrument Settings ---
Carrier: H2Ar @ 50.00 (None @ 100.00)
Loop: None @ 10.00 (None @ 100.00)
Prep.: None @ 10.00 (None @ 100.00)
(Bypass) (Bypass) (Fill) (Analyze) Trap
Filaments:245.0 °C (Disabled)
1.03 Wait --- Wait ---
Wait 10.00 min.
1.04 Wait --- Wait ---
Wait until baseline and temperatures are stable.
1.05 Start Recording --- Start Recording ---
One measurement every 0.20 s
Set external trigger: No
1.06 Temperature Ramp --- Temperature Ramp ---
Type: Sample
Temperature: 400.0 °C
Ramp rate: 10.0 °C/min
Hold time: 5.00 min
1.07 Stop Recording --- Stop Recording ---
Termination --- Termination ---
Carrier: Ar @ 10.00 (H2Ar @ 50.00)
(Bypass) (Bypass) (Fill) Prepare (Trap)
Port: 60.0 °C (110.0 °C)
Sample: Ambient (400.0 °C)
Rate: Ambient (10.0 °C/min)
Filaments:Disabled (245.0 °C)
Adsorptive Properties
Adsorptive: Hydrogen-Argon (H2Ar)
Maximum manifold pressure: 123.323 kPa
Molecular cross-sectional area: 0.123 nm²
Adsorbate molecular weight: 2.02
Relative thermal conductivity: 1.40
Gas blend: Yes
Inert gas: Argon
Active gas: Hydrogen
% Active Concentration 9.998 %
Fluid properties: H:\FPI\fpiv7\hydrogen.fpi
Adsorptive: Argon (Ar)
Report Options
Report options: Report Options
Summary: Yes
BET Surface Area: No
Pulse Chemisorption: No
First Order Kinetics: No
Loop Calibration: No
Active Surface Area: No
Signal and Temperature vs. Time: Yes
Signal and Temperature vs. Time
Show peak marks: Yes
X-axis: Time
Autoscale: Yes
Y-axis: Signal
Autoscale: Yes
Experiments:
1: CuO TPR 50 sccm H2Ar Yes
Active Gas Flow Rate vs. Temperature 1: Yes
Active Gas Flow Rate vs. Temperature 1
Show peak marks: Yes
X-axis: Temperature
Autoscale: Yes
Y-axis: Active Gas Flow Rate
Autoscale: Yes
Experiments:
1: CuO TPR 50 sccm H2Ar Yes
Signal vs. Temperature 1: No
Active Gas Flow Rate vs. Time 1: No
Active Gas Flow Rate vs. Temperature 2: No
Signal vs. Time: No
Signal vs. Temperature 2: No
Active Gas Flow Rate vs. Time 2: No
Active Gas Flow Rate vs. Temperature 3: No
Signal and Active Gas Flow Rate vs. Time: No
Advanced Reports: No
Options Report: No
Sample Log: Yes
Peak Detection/Integration Options
Baseline mode: Best fit baseline
Minimum peak height: 0.25 % F.S.
Peak smoothing: 0 points
Sensitivity: 1.0e-02 % F.S.
Maximum shoulder ratio: 33%
Maximum group separation: 33%
Minimum peak area: 1.0 % F.S.·min
Maximum baseline slope: 0.1 % F.S./sec
Collected Data
Collected Data
Serial number: 002
Start time: 12/10/2020 4:30:04 PM
Stop time: 12/10/2020 5:29:57 PM
Ambient temperature: 25.0 °C
Atmospheric pressure: 101.3 kPa
p° of N2: 103.3249 kPa
Tables have been truncated to 1000 entries for preview.
Consider restricting the time range, using a larger time interval, or exporting directly to a file.
CuO TPR 50 sccm H2Ar
Experiment ID: 1: CuO TPR 50 sccm H2Ar
Calibration: (AutoChem_III_0002) 10% H2/Ar 50cc 121020
Analysis type: Temperature Programmed Desorption
Measured flow rate: 50.00000 cm³ STP/min
Active concentration % at time 0: 9.998 %
Physical injection volume: 1.0000 mL
Use fit peaks: No
Start time: 0.00 min
Stop time: 43.15 min
CuO TPR 50 sccm H2Ar
Temperature
Start Stop at
Peak Time Time Maximum Quantity
Number (min) (min) (°C) (cm³ STP)
-----
1 3.55 33.93 207.42 15.383484
CuO TPR 50 sccm H2Ar
Carrier Loop
Flow Flow
Rate Rate Reflux
Time Temperature Signal (a Injection (cm³ (cm³ Temperature
(min) (°C) u ) Event STP/min) STP/min) (°C)
-------
0.0000 27.3 0.020317575 0 50.00 0.03 24.3
0.0033 27.3 0.020331932 0 50.00 0.03 24.3
0.0067 27.3 0.020329252 0 50.00 0.03 24.3
0.0100 27.3 0.020342696 0 50.00 0.03 24.3
0.0133 27.3 0.020332888 0 50.00 0.03 24.3
0.0167 27.3 0.020323444 0 50.00 0.03 24.3
0.0200 27.3 0.020320816 0 50.00 0.03 24.3
0.0233 27.3 0.020332487 0 50.00 0.03 24.3
0.0267 27.3 0.020331409 0 50.00 0.03 24.3
0.0300 27.3 0.020303261 0 50.00 0.03 24.3
0.0333 27.3 0.020322692 0 50.00 0.03 24.3
0.0367 27.3 0.020317623 0 50.00 0.03 24.3
0.0400 27.3 0.020327993 0 50.00 0.03 24.3
0.0433 27.3 0.020315453 0 50.00 0.03 24.3
0.0467 27.3 0.020320794 0 50.00 0.03 24.3
0.0500 27.3 0.020323554 0 50.00 0.03 24.3
0.0533 27.3 0.020323807 0 50.00 0.03 24.3
0.0567 27.3 0.020352364 0 50.00 0.03 24.3
0.0600 27.3 0.020323513 0 50.00 0.03 24.3
0.0633 27.3 0.020334244 0 50.00 0.03 24.3
0.0667 27.3 0.020322597 0 50.00 0.03 24.3
0.0700 27.3 0.020311031 0 50.00 0.03 24.3
0.0733 27.3 0.020342128 0 50.00 0.03 24.3
0.0767 27.3 0.020313352 0 50.00 0.03 24.3
0.0800 27.3 0.020326018 0 50.00 0.03 24.3
0.0833 27.3 0.02031542 0 50.00 0.03 24.3
0.0867 27.3 0.020323347 0 50.00 0.03 24.3
0.0900 27.3 0.020325938 0 50.00 0.03 24.3
0.0933 27.3 0.020327948 0 50.00 0.03 24.3
0.0967 27.3 0.020308368 0 50.00 0.03 24.3
0.1000 27.3 0.020344859 0 50.00 0.03 24.3
Copyright © 2022 - 2024. Micromeritics Instrument Corporation. All rights reserved.
|
|
|
|
|